Study on optimization parameters of spray drying and quality evaluation of Channa argus head soup drying product
-
摘要: 为满足消费者对美味鱼汤产品的需求,提高乌鳢 (Channa argus) 加工副产物的利用价值,以前期制备的乌鳢鱼头汤为原料,用麦芽糊精作助干剂,采用喷雾干燥法制备乌鳢鱼头汤粉末,以干燥粉末的水分质量分数、色泽、溶解性、堆积密度、冲调时间以及粘壁情况为评价指标对喷雾干燥工艺优化进行研究。结果表明,麦芽糊精能够有效提高喷雾干燥的集粉率、粉体亮度、溶解性,改善粘壁情况;麦芽糊精质量浓度为15 g·L − 1、喷雾干燥进风温度为170 ℃、进料速度为6 mL·min − 1时喷雾效果和产品品质最佳,所制得的乌鳢鱼头汤粉末具有含水量较低、堆积密度较大、溶解度较高、吸湿性较低和颗粒均匀等特性。综上,喷雾干燥法可作为乌鳢鱼头汤粉末的制备方法。Abstract: In order to meet consumers' demand for delicious fish soup products, and improve the utilization value of Channa argus processing by-products, we prepared the fish head soup by spray drying method using C. argus head soup as raw material and maltodextrin as a drying aid. The optimization of spray drying technology was carried out by analyzing the water mass fraction, color, solubility, bulk density, time of punching and viscosity of dry powder. The results show that maltodextrin could increase the spray drying rate, powder brightness and solubility effectively, and improve the adhesive condition. With the maltodextrin addition amount of 15 g·L − 1, spray drying inlet temperature of 170 ℃ and feeding speed of 6 mL·min − 1, the spray effect and product quality were the best. The prepared fish head soup powder contained low water content, large packing density, high solubility, low moisture absorption and uniform particle size. In conclusion, spray drying method can be used as a preparation method for fish head soup.
-
Key words:
- Channa argus head soup /
- Spray drying /
- Parameter optimization /
- Maltodextrin /
- Quality evaluation
-
表 1 助干剂对产品喷雾干燥的影响
Table 1. Effect of carrier on spray drying of product
麦芽糊精质量浓度
Addition of
maltdextrin/(g·L−1)集粉率
Powder collection
rate/%水分质量分数
Moisture
mass fraction/%堆积密度
Bulk density/
(g·mL−1)冲调时间
t/s亮度
L*红绿色度
a*蓝黄色度
b*白度
Brightness粘壁情况
Wall
sticking0 13.5a 4.84b 0.365a 117d 50.13b −0.14d 7.01c 49.64b 粘壁严重 5 19.9b 6.07c 0.456d 104c 48.00a −0.31a 3.39b 47.89a 粘壁严重 10 38.5c 5.08b 0.441c 84b 48.63a −0.26b 2.55a 48.57a 部分粘壁 15 37.7c 4.17a 0.434b 77a 51.49b −0.35a 2.39a 51.43b 轻微粘壁 20 39.2c 4.03a 0.429b 74a 50.60b −0.22c 2.13a 50.55b 几乎不粘壁 注:同一列标注不同小写字母表示组间存在显著差异(P<0.05);下表同此。 Note: Different lowercase letters within the same column indicate significant difference between groups (P<0.05). The same case in the following tables. 表 2 进风温度对产品喷雾干燥的影响
Table 2. Effect of inlet air temperature on spray drying of product
温度
Temperature/
℃集粉率
Powder collection
rate/%水分质量分数
Moisture
mass fraction/%堆积密度
Bulk density/
(g·mL−1)冲调时间
t/min亮度
L*红绿色度
a*蓝黄色度
b*白度
Brightness粘壁情况
Wall sticking160 41.86c 6.11c 0.390b 1.40b 54.59b −0.38b 4.29a 54.39b 部分粘壁 170 43.02d 4.77a 0.362b 1.32a 56.29c −0.48a 4.66b 56.04b 轻微粘壁 180 37.70b 6.09c 0.401c 1.29a 51.49a −0.32b 4.30a 51.29a 轻微粘壁 190 35.41a 4.97b 0.304a 1.46c 51.50a −0.47a 5.34c 51.20a 少量粘壁 表 3 进料速度对产品喷雾干燥的影响
Table 3. Effect of feeding speed on spray drying of product
进料速度
Processing velocity/
(mL·min−1)集粉率
Powder collection
rate/%水分质量分数
Moisture
mass fraction/%堆积密度
Bulk density/
(g·mL−1)冲调时间
t/s亮度
L*红绿色度
a*蓝黄色度
b*白度
Brightness粘壁情况
Wall sticking6 44.55c 3.91a 0.301b 58b 52.75a −0.30b 4.01b 52.58a 轻微粘壁 9 40.64b 4.54b 0.297b 47a 55.80b −0.39a 3.84a 55.63b 部分粘壁 12 42.29b 4.93c 0.296b 75d 53.53a −0.36ab 4.36c 53.32a 轻微粘壁 15 34.99a 5.41d 0.287a 65c 54.89b −0.43a 3.87ab 54.72b 严重粘壁 表 4 喷雾干燥的乌鳢鱼头汤粉品质指标
Table 4. Quality index of C. argus head soup powder made by spray drying
水分质量分数
Moisture mass fraction/%堆积密度
Bulk density/(g·mL−1)溶解度
Solubility/[g·(100 mL)−1]吸湿性
Hygroscopicity/[g·(100 g)−1]4.03±0.15 0.54±0.09 99.13±1.98 24.47±1.65 表 5 粉末粒径和跨度指数
Table 5. Particle sizes and span index of powder
粉末粒径 Particle size/μm 跨度指数
SpanD[4,3] D90 D50 D10 2.84±1.15 5.43±0.57 2.80±0.07 0.87±0.01 1.63±0.15 -
[1] WANG R, MIN Z, MUJUMDAR A S. Effect of food ingredient on microwave freeze drying of instant vegetable soup[J]. LWT, 2010, 43(7): 1144-1150. doi: 10.1016/j.lwt.2010.03.007 [2] LIU W, ZHANG M, ADHIKARI B, et al. A novel strategy for improving drying efficiency and quality of cream mushroom soup based on microwave pre-gelatinization and infrared freeze-drying[J]. Innov Food Sci Emerg, 2020, 66(4): 102516. [3] SINGH S, GHOSH S, PATIL G R. Development of a mushroom-whey soup powder[J]. Int J Food Sci Tech, 2010, 38(2): 217-224. [4] 黄卉, 李来好, 杨贤庆, 等. 喷雾干燥微胶囊化罗非鱼油的研究[J]. 南方水产, 2009, 5(5): 19-23. [5] 郑唯, 朱丹, 牛广财, 等. 助干剂对毛酸浆喷雾干燥粉集粉率及性质的影响[J]. 食品工业, 2018, 39(8): 144-147. [6] TEO A, LAM Y, LEE S J, et al. Spray drying of whey protein stabilized nanoemulsions containing different wall materials-maltodextrin or trehalose[J]. LWT, 2021, 136: 110344. doi: 10.1016/j.lwt.2020.110344 [7] 李秀军, 王彦民, 杨利刚, 等. 活性乳酸菌酸奶粉加工关键技术研究[J]. 食品研究与开发, 2017, 38(24): 109-117. doi: 10.3969/j.issn.1005-6521.2017.24.022 [8] CAI Y, CORKE H. Production and properties of spray-dried Amaranthus betacyanin pigments[J]. J Food Sci, 2010, 65(7): 1248-1252. [9] 马占强. 雪莲果粉干燥工艺及贮藏稳定性研究 [D]. 淄博: 山东理工大学, 2013: 47-56. [10] SAÉNZ C, TAPIA S, CHÁVEZ J, et al. Microencapsulation by spray drying of bioactive compounds from cactus pear (Opuntia ficusindica)[J]. Food Chem, 2009, 114(2): 616-622. doi: 10.1016/j.foodchem.2008.09.095 [11] CANO-CHAUCA M, STRINGHETA P C, RAMOS A M, et al. Effect of the carriers on the microstructure of mango powder obtained by spray drying and its functional characterization[J]. Innov Food Sci Emerg, 2005, 6(4): 420-428. doi: 10.1016/j.ifset.2005.05.003 [12] QUEK S Y, CHOK N K, SWEDLUND P E, et al. The physicochemical properties of spray-dried watermelon powders[J]. Chem Eng Process, 2007, 46(5): 386-392. doi: 10.1016/j.cep.2006.06.020 [13] JAFARI S M, GHALEGI M, DEHNAD D. Influence of spray drying on water solubility index, apparent density, and anthocyanin content of pomegranate juice powder[J]. Powder Techol, 2017, 311: 59-65. doi: 10.1016/j.powtec.2017.01.070 [14] 黄绍天, 王步江. 卤料调味粉喷雾干燥工艺研究[J]. 中国调味品, 2019, 44(5): 159-162. [15] 蒋丽施, 孟晓, 李瑶, 等. 白乌鱼方便鱼汤粉加工工艺研究[J]. 中国调味品, 2020, 45(10): 85-87,92. doi: 10.3969/j.issn.1000-9973.2020.10.018 [16] MUZAFFAR K, KUMAR P. Parameter optimization for spray drying of tamarind pulp using response surface methodology[J]. Powder Techol, 2015, 279: 179-184. doi: 10.1016/j.powtec.2015.04.010 [17] ZHANG Z, SONG H, ZHEN P, et al. Characterization of stipe and cap powders of mushroom (Lentinus edodes) prepared by different grinding methods[J]. J Food Eng, 2012, 109(3): 406-413. doi: 10.1016/j.jfoodeng.2011.11.007 [18] HUPPERTZ T. Analytical methods for food and dairy powders[J]. Int Dairy J, 2012, 27(1): 103. [19] FERNANDES R V, BORGES S V, BOTREL D A. Gum arabic/starch/maltodextrin/inulin as wall materials on the microencapsulation of rosemary essential oil[J]. Carbohyd Polym, 2014, 101: 524-532. doi: 10.1016/j.carbpol.2013.09.083 [20] 朱琳芳. 方便鱼汤加工技术研究与开发[D]. 无锡: 江南大学, 2012: 27-29. [21] 宋玲霞, 陈义伦, 马超, 等. 干燥方式对枣粉物理特性的影响[J]. 食品与发酵工业, 2014, 40(12): 89-93. [22] 付露莹, 原双进, 陈浩, 等. 喷雾干燥与真空冷冻干燥对核桃粕红枣复合粉品质的影响[J]. 食品与机械, 2019, 35(1): 210-214. [23] VBA B, LRGA B, RCDSA B, et al. Production and characterization of pineapple-mint juice by spray drying[J]. Powder Technol, 2020, 375: 409-419. doi: 10.1016/j.powtec.2020.08.012 [24] TONON R V, BRABET C, HUBINGER M D. Influence of process conditions on the physicochemical properties of açai (Euterpe oleraceae Mart. ) powder produced by spray drying[J]. J Food Eng, 2008, 88(3): 411-418. doi: 10.1016/j.jfoodeng.2008.02.029 [25] FERRARI C C, GERMER S, ALVIM I D, et al. Influence of carrier agents on the physicochemical properties of blackberry powder produced by spray drying[J]. Int J Food Sci Tech, 2012, 47(6): 1237-1245. doi: 10.1111/j.1365-2621.2012.02964.x [26] RODRÍGUEZ-HERNÁNDEZ G, GONZÁLEZ-GARCÍA R, GRAJALES-LAGUNES A, et al. Spray-drying of cactus pear juice (Opuntia streptacantha): effect on the physicochemical properties of powder and reconstituted product[J]. Dry Technol, 2005, 23(4): 955-973. doi: 10.1080/DRT-200054251 [27] ZOTARELLI M F, SILVA V M, DURIGON A, et al. Production of mango powder by spray drying and cast-tape drying[J]. Powder Technol, 2017, 305: 447-454. doi: 10.1016/j.powtec.2016.10.027 [28] SARRATE R, TICÓ J, MIARRO M, et al. Modification of the morphology and particle size of pharmaceutical excipients by spray drying technique[J]. Powder Technol, 2015, 270: 244-255. doi: 10.1016/j.powtec.2014.08.021 [29] GUO J, LI P, KONG L, et al. Microencapsulation of curcumin by spray drying and freeze drying[J]. LWT, 2020, 132: 109892. doi: 10.1016/j.lwt.2020.109892 -